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Lofdal Heavy Rare Earth Deposit: Successful Hydrometallurgical Test Work Results in Highly Efficient Process to Produce a Market Ready >98% Rare Earth Oxide Product

Lofdal Heavy Rare Earth Deposit: Successful Hydrometallurgical Test Work Results in Highly Efficient Process to Produce a Market Ready >98% Rare Earth Oxide Product

洛夫达尔重稀土矿床:成功的湿法冶金测试工作带来了生产市场准备率大于98%的稀土氧化物产品的高效工艺
Accesswire ·  2021/10/07 09:52

HALIFAX, NS / ACCESSWIRE / October 7, 2021 / Namibia Critical Metals Inc. ("Namibia Critical Metals" or the "Company" or "NMI") (TSXV:NMI) is pleased to provide an update on the development of the Lofdal Heavy Rare Earth project since granting of the Mining Licence in July this year. The Lofdal Heavy Rare Earth Deposit is one of only two primary xenotime projects under development in the world. The deposit has the potential for significant production of dysprosium and terbium, the two most valuable heavy rare earth elements used in high powered magnets and other high-tech applications. The Project is being developed in joint venture with Japan Oil, Gas and Metals National Corporation ("JOGMEC") targeting a long term, sustainable supply of heavy rare earths to Japan.

哈利法克斯,NS/ACCESSWIRE/2021年10月7日/纳米比亚关键金属公司(“纳米比亚关键金属”或“公司”或“NMI”)(多伦多证券交易所股票代码:NMI)很高兴提供自今年7月授予采矿许可证以来洛夫达尔重稀土项目开发的最新情况。洛夫达尔重稀土矿床是世界上仅有的两个正在开发的主要Xe-time项目之一。该矿床具有大量生产镝和铽的潜力,这两种最有价值的重稀土元素用于大功率磁体和其他高科技应用。该项目正在与日本石油、天然气和金属国家公司(JOGMEC)合资开发,目标是向日本长期、可持续地供应重稀土。

The Company has successfully completed hydrometallurgical test work to develop a flowsheet capable of producing a high-grade rare-earth oxide product from a xenotime flotation concentrate. The Company's lead metallurgical consultants at SGS Minerals Services Canada (SGS) have simplified the final process stage with an acid bake to crack the mineral xenotime, to purify the pregnant leach solution and to precipitate a rare earth oxalate, which is subsequently calcined to form a product containing >98% total rare earth oxides (TREO). The acid bake process and concurrent removal of impurities is highly efficient and resulted in a 95% recovery of Dysprosium and Terbium in the leaching operation of the processing flow sheet. The high-quality product is practically free of typical deleterious elements like thorium and uranium (<3 ppm combined U+Th).

该公司已成功完成湿法冶金试验工作,开发了一套能够从混合浮选精矿中生产高品位稀土氧化物产品的工艺流程。公司在SGS加拿大矿产服务公司(SGS)的首席冶金顾问通过酸焙简化了最后的流程阶段,通过酸焙烧来裂解矿物,提纯怀孕的浸出液,沉淀出稀土草酸盐,然后进行煅烧,形成总稀土氧化物(TREO)>98%的产品。酸性焙烧过程和同时去除杂质的效率很高,在工艺流程的浸出操作中,镝和铽的回收率达到95%。高质量的产品几乎不含钍、铀等典型的有害元素。

Darrin Campbell, President of Namibia Critical Metals stated:

纳米比亚关键金属公司总裁达林·坎贝尔表示:

These very positive test results are another big milestone for the Lofdal project and show that we are on the right path towards establishing that Lofdal can produce a valuable heavy rare earth product. This will allow us to advance an updated assessment of large-scale and integrated rare earth production towards a high purity Rare Earth Oxide product in Namibia. This would result in further value addition in Namibia and puts the country on the global map of rare earth supply strategies."

这些非常积极的测试结果是洛夫达尔项目的又一个重大里程碑,表明我们正走在正确的道路上,证明洛夫达尔可以生产有价值的重稀土产品。这将使我们能够推进对纳米比亚高纯度稀土氧化物产品的大规模综合稀土生产的最新评估。这将进一步增加纳米比亚的附加值,并使该国在全球稀土供应战略地图上占有一席之地。“

Hydrometallurgical test work and results

湿法冶金试验工作及结果

Two flotation concentrates produced by processing of bulk samples from the Lofdal deposit were tested at the laboratories of SGS in Lakefield, Ontario, to determine the potential for producing a marketable rare earth product with minimal impurities. Previous hydrometallurgical test work had focused on more costly caustic cracking following gangue acid leach. The comprehensive test work at SGS has demonstrated the acid bake route is preferred due to lower reagent costs and higher recovery of the heavy rare earths.

在安大略省莱克菲尔德的SGS实验室对洛夫达尔矿床大宗样品加工生产的两种浮选精矿进行了测试,以确定生产杂质最少的适销对路稀土产品的潜力。以前的湿法冶金测试工作主要集中在煤矸石酸浸出后成本更高的腐蚀性裂解上。SGS的综合试验工作表明,酸性焙烧路线是首选的,因为试剂成本较低,重稀土的回收率较高。

A total of 12 acid bake and water leach tests were completed throughout the test program to investigate the dissolution of rare earth elements (REE) and the behaviour of gangue minerals through the addition of sulphuric acid at elevated temperatures (200-300°C). Optimum results were achieved using an acid addition of 1250 kg/t H2SO4 at 300°C followed by a water leach at 20% solids by weight at 25°C. Under these conditions, the tests showed very good REE recoveries with 97-98% for yttrium, 95% for dysprosium and 94-95% for terbium.

整个测试项目共完成了12次酸焙烧和水浸试验,以研究稀土元素(REE)的溶解以及在高温(200-300°C)下添加硫酸对脉石矿物行为的影响。在酸添加量为1250 kg/tH的情况下获得最佳结果2所以4在300°C下,25°C下20%固体含量的水浸出,获得了很好的稀土回收率,钇的回收率为97-98%,镝的回收率为95%,铽的回收率为94-95%。

Table 1: Elemental composition of the calcined oxalate

表1:煅烧草酸盐的元素组成

Impurity removal test work using magnesium carbonate and hydrogen peroxide resulted in maximum precipitation of iron and thorium from the pregnant leach solution while minimizing REE co-precipitation. An intermediate and impure REE precipitate was produced via the addition of soda ash (sodium carbonate) solution.

使用碳酸镁和过氧化氢进行的除杂试验工作使铁和钍从怀孕的浸出液中得到最大限度的沉淀,同时最大限度地减少了稀土元素的共沉淀。通过加入纯碱(碳酸钠)溶液,生成中间不纯的稀土沉淀物。

The intermediate REE precipitate was re-leached in sulphuric acid using a two-stage sulphuric acid process at 50°C to achieve a pulp pH of around 3.5. This step resulted in the production of a concentrated REE liquor representing 99% of the available REE and also rejected 94% of the thorium, 85% of the aluminum, and 99% of the remaining iron.

中间稀土沉淀在50°C下采用两段硫酸工艺在硫酸中重新浸出,以达到矿浆pH值3.5左右。这一步骤产生了浓缩的稀土溶液,相当于有效稀土的99%,同时也排除了94%的钍、85%的铝和99%的剩余铁。

To remove residual uranium and thorium, the re-leach liquor was processed through sequential ion exchange (Purolite A660) and solvent extraction (0.5% Primene JMT, 2.5% isodecanol in Aromatic 150ND) steps to selectively remove uranium and thorium from the REE liquor. Consequently, 99.9% of the uranium was removed in the IX contacts. A significant fraction (94%) the thorium was also removed in the IX steps and 75% of the remaining thorium was removed in the solvent extraction steps. The practically thorium-free raffinate from the solvent extraction step advanced to final REE precipitation with oxalic acid and calcination of the REE oxalate.

为了去除残留的铀和钍,再浸出液经过顺序离子交换(Purolite A660)和溶剂萃取(0.5%伯门烯JMT,2.5%异癸醇在芳香族150ND中)步骤,选择性地从稀土溶液中脱除铀和钍。因此,99.9%的铀在IX触点中被清除。很大一部分(94%)的钍也在第IX步中被去除,剩余的75%的钍在溶剂萃取步骤中被除去。溶剂萃取后的实际无钍残液,经草酸沉淀、焙烧后得到稀土草酸盐。

In the REE oxalate precipitation step, all REE were precipitated with minimal co-precipitation of impurities such as sodium, magnesium, silica and calcium. The final REE oxalate was calcined and produced a final solid containing 98.1% total rare earth oxides (TREO) or 86.2% of heavy rare earth oxides (HREO). High leach extractions of ~95% were achieved in the test program and REE losses in the REE recovery steps (as shown in Figure 1) are expected to be minimal.

在稀土草酸盐析出步骤中,所有稀土元素都被沉淀出来,钠、镁、硅和钙等杂质的共沉淀很少。最终的稀土草酸盐经煅烧后得到总稀土氧化物(TREO)98.1%或重稀土氧化物(HREO)86.2%的最终固体。在试验计划中实现了~95%的高浸出率,REE回收步骤(如图1所示)中的稀土损失预计最小。

Figure 1: Hydrometallurgical process flowsheet developed using Lofdal flotation concentrate

图1:使用洛夫达尔浮选精矿开发的湿法冶金工艺流程

While the results are extremely positive, there remains room to optimise these processes regarding OPEX and CAPEX as well as recoveries. This final optimisation on flotation concentrate produced from the currently mined bulk samples is planned for 2022.

虽然结果非常积极,但在运营支出和资本支出以及回收方面,仍有优化这些流程的空间。从目前开采的散装样品生产的浮选精矿的最终优化计划于2022年进行。

Planning for further value addition in Namibia

在纳米比亚规划进一步增值

The positive hydrometallurgical test results allow for planning of value addition beyond the production of a xenotime concentrate at the Lofdal Mine providing for a win-win for the country and the company.

积极的湿法冶金测试结果允许计划在洛夫达尔矿生产稀土精矿以外的附加值,为国家和公司带来双赢。

The addition of a hydrometallurgical plant would create further jobs in the southern Kunene Region of Namibia, and provides a marketable product for export as the rare earth oxalate with thorium and uranium levels below 3 ppm would be acceptable for import into Japan without restrictions or penalties.

增加一家湿法冶金厂将在纳米比亚库内内南部地区创造更多就业机会,并为出口提供适销对路的产品,因为钍和铀含量低于3ppm的稀土草酸盐可以不受限制或处罚地进口到日本。

About Japan Oil, Gas and Metals National Corporation (JOGMEC)

关于日本石油、天然气和金属国家公司(JOGMEC)

JOGMEC is a Japanese government independent administrative agency which among other things seeks to secure stable resource supplies for Japan. JOGMEC has a strong reputation as a long term, strategic partner in mineral projects globally. The mandated areas of responsibilities within JOGMEC relate to oil and natural gas, metals, coal and geothermal energy. JOGMEC facilitates opportunities with Japanese private companies to secure supplies of natural resources for the benefit of the country's economic development.

JOGMEC是日本政府的独立行政机构,其主要任务是确保日本稳定的资源供应。JOGMEC作为全球矿产项目的长期战略合作伙伴而享有盛誉。JOGMEC的授权职责领域涉及石油和天然气、金属、煤炭和地热能源。JOGMEC促进了与日本私营公司的机会,以确保自然资源的供应,从而造福于日本的经济发展。

Rare earths are of critical importance to Japanese industrial interests and JOGMEC has extensive experience with all aspects of the sector. JOGMEC provided Lynas with US$250,000,000 in loans and equity in 2011 to ensure supplies of the Light Rare Earths metals suite to the Japanese industry.

稀土对日本的工业利益至关重要,JOGMEC在该行业的各个方面都有丰富的经验。JOGMEC于二零一一年向Lynas提供250,000,000美元贷款及股权,以确保向日本业界供应轻稀土金属套件。

The Company currently owns a 95% interest in the Lofdal project with the remaining 5% held for the benefit of historically disadvantaged Namibians. The terms of the JOGMEC joint venture agreement with the Company stipulate that JOGMEC provides $3,000,000 in Term 1 and $7,000,000 in Term 2 to earn a 40% interest in the Lofdal project. Term 3 calls for a further $10,000,000 of expenditures to earn an additional 10% interest. JOGMEC can also purchase another 1% for $5,000,000 and has first right of refusal to fully fund the project through to commercial production and to purchase all production at market prices. The collective interests of NMI and historically disadvantaged Namibians cannot be diluted below a 26% carried working interest upon payment of $5,000,000 to JOGMEC for the dilution protection. The JV Agreement is structured such that no NMI equity will be issued and it is totally non-dilutive to NMI shareholders. To date, JOGMEC, has funded Term 1 and 2 expenditures totaling $6,600,000.

该公司目前在Lofdal项目中拥有95%的权益,其余5%的权益是为历史上处于不利地位的纳米比亚人的利益而持有的。JOGMEC与公司的合资协议条款规定,JOGMEC在第一期提供300万美元,在第二期提供700万美元,以赚取洛夫达尔项目40%的权益。条款3要求再增加1000万美元的支出,以赚取额外10%的利息。JOGMEC还可以以500万美元的价格再购买1%的股份,并有权优先拒绝为该项目提供全额资金,直至商业化生产,并以市场价格购买所有产品。在向JOGMEC支付500万美元用于稀释保护后,NMI和历史上处于不利地位的纳米比亚人的集体利益不能稀释到26%的附带工作权益以下。合营协议的结构将不会发行任何NMI股权,且对NMI股东完全不具摊薄作用。到目前为止,JOGMEC已经为第一和第二期支出提供了总计660万美元的资金。

About Namibia Critical Metals Inc.

关于纳米比亚关键金属公司

Namibia Critical Metals Inc. holds a diversified portfolio of exploration and advanced stage projects in the country of Namibia focused on the development of sustainable and ethical sources of metals for the battery, electric vehicle and associated industries. The two advanced stage projects in the portfolio are Lofdal and Epembe. The Company also holds significant land positions in areas favourable for gold mineralization.

纳米比亚关键金属公司在纳米比亚拥有多元化的勘探和高级阶段项目组合,专注于为电池、电动汽车和相关行业开发可持续和符合道德标准的金属来源。该投资组合中的两个高级阶段项目是Lofdal和Epembe。该公司还在有利于金矿成矿的地区持有大量土地头寸。

Figure 2: Location of Namibia Critical Metals' projects highlighting position of gold projects (Erongo, Otjiwarongo and Grootfontein) in relation to important gold projects within the Navachab-Otjikoto gold belt

图2:纳米比亚关键金属项目的位置突出了黄金项目(Erongo、Otjiwarongo和Grootfontein)与Navachab-Otjikoto金矿带内重要黄金项目的关系

Heavy Rare Earths: The Lofdal Dysprosium-Terbium Project is the Company's most advanced project being fully permitted with a Mining Licence (ML 200) issued in 2021. The project is being developed in joint venture with Japan Oil, Gas and Metals National Corporation ("JOGMEC") to provide a sustainable supply of heavy rare earths to Japan, most notably dysprosium and terbium.

重稀土:这个洛夫达尔镝-铽项目该公司最先进的项目是否获得了2021年颁发的采矿许可证(ML 200)的全面许可。该项目正在与日本石油、天然气和金属国家公司(JOGMEC)合资开发,以向日本提供可持续的重稀土供应,最明显的是镝和铽。

Gold: The Company's Exclusive Prospecting Licenses ("EPLs") prospective for gold are located in the Central Namibian Gold Belt which hosts a number of significant orogenic gold deposits including the Navachab Gold Mine, the Otjikoto Gold Mine and more recently the discovery of the Twin Hills deposit. At the Erongo Gold Project, stratigraphic equivalents to the meta-sediments hosting the recent Osino gold discovery at Twin Hills have been identified and soil surveys are progressing over this highly prospective area. The Grootfontein Base Metal and Gold Project has potential for magmatic copper-nickel mineralization, Mississippi Valley-type zinc-lead-vanadium mineralization and Otjikoto-style gold mineralization. Detailed interpretation of geophysical data and regional geochemical soil sampling have identified first gold targets, with the first targets currently being drill-tested.

黄金:公司的独家金矿勘探许可证(“EPL”)位于纳米比亚中部金矿带,该地区拥有许多重要的造山带金矿,包括Navachab金矿、Otjikoto金矿以及最近发现的Twin Hills金矿。在Erongo黄金项目与最近在双子山发现Osino金矿的变质沉积物相对应的地层已经确定,这一极具远景的地区正在进行土壤调查。这个Grootfontein贱金属和黄金项目具有岩浆铜镍成矿、密西西比谷型锌铅钒成矿和大藤式金矿化的潜力。对地球物理数据的详细解释和区域地球化学土壤采样已经确定了第一批金矿目标,第一批目标目前正在进行钻探测试。

Tantalum-Niobium: The Epembe Tantalum-Niobium-Uranium Project is at an advanced stage with a well-defined, 10 km long carbonatite dyke that has been delineated by detailed mapping and radiometric surveys and over 11,000 meters of drilling. Preliminary mineralogical and metallurgical studies including sorting tests (XRT), indicate the potential for significant physical upgrading. Further work will be undertaken to advance the project to a preliminary economic assessment stage.

钽铌:这个Epembe钽铌铀项目该项目已进入后期阶段,有一条10公里长的碳酸盐岩堤坝,已通过详细的测绘和放射性测量以及超过11,000米的钻探进行了圈定。初步的矿物学和冶金研究,包括分选试验(XRT),表明有可能进行重大的物理升级。将进一步开展工作,使该项目进入初步经济评估阶段。

Copper-Cobalt: The Kunene Copper-Cobalt Project comprises a large area of favorable stratigraphy along strike of the Opuwo cobalt-copper-zinc deposit. Secondary copper mineralization over a wide area points to preliminary evidence of a regional-scale hydrothermal system. Exploration targets on EPLs held in the Kunene project comprise direct extensions of the cobalt-copper mineralization to the west, sediment-hosted copper, orogenic copper, and stratabound manganese and zinc-lead mineralization.

铜-钴:这个库内纳铜钴项目包括沿欧普沃钴铜锌矿床走向的大片有利地层。大面积的次生铜矿化表明存在区域规模的热液系统的初步证据。库内纳项目中EPL的勘探目标包括钴铜矿向西的直接延伸、沉积物容矿铜、造山铜以及层控锰和锌铅矿化。

The common shares of Namibia Critical Metals Inc. trade on the TSX Venture Exchange under the symbol "NMI".

纳米比亚关键金属公司的普通股在多伦多证券交易所创业板交易,代码为“NMI”。

Micheal Archer of SGS is the Company's Qualified Person and has reviewed and approved the scientific and technical information in this press release.

SGS的Michel Archer是该公司的合格人员,并已审核并批准了本新闻稿中的科学技术信息。

Neither the TSX Venture Exchange nor its Regulation Services Provider (as that term is defined in the policies of the TSX Venture Exchange) accepts responsibility for the adequacy or accuracy of this release.

多伦多证券交易所创业板交易所及其监管服务提供商(该术语在多伦多证券交易所创业板政策中定义)均不对本新闻稿的充分性或准确性承担责任。

For more information please contact -

如需更多信息,请联系-

Namibia Critical Metals Inc.
Darrin Campbell, President
Tel: +01 (902) 835-8760
Fax: +01 (902) 835-8761
Email: Info@NamibiaCMI.com
Web site: www.NamibiaCriticalMetals.com

纳米比亚关键金属公司。达林·坎贝尔(Darrin Campbell)总统电话:+01(902)835-8760传真:+01(902)835-8761电子邮件:info@纳米biaCMI.com网址:www.纳米biaCriticalMetals.com

The foregoing information may contain forward-looking information relating to the future performance of Namibia Critical Metals Inc. forward-looking information, specifically, that concerning future performance, is subject to certain risks and uncertainties, and actual results may differ materially. These risks and uncertainties are detailed from time to time in the Company's filings with the appropriate securities commissions.

上述信息可能包含有关纳米比亚关键金属公司未来业绩的前瞻性信息。前瞻性信息,特别是有关未来业绩的前瞻性信息,可能会受到某些风险和不确定性的影响,实际结果可能与此大不相同。这些风险和不确定因素在公司不时向适当的证券委员会提交的文件中有详细说明。

SOURCE: Namibia Critical Metals Inc.

资料来源:纳米比亚关键金属公司。


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